I decided to change
my project idea to something that has to do with my degree (Chemical
Engineer). I was very confused at first, so I brainstormed with my
grandfather who is a chemist, and he told me to work on improving a
system of essential oil extraction. In the laboratory, we are often
working with steam distillation (a method for distilling compounds
which are heat-sensitive). I have decided to use this method to
separate the essential oils. By the end of the process, we will be able
to separate the oil from the water. Usually we do it by using
micropipettes once the oil floats to the top and the water sinks to the
bottom.
In steam distillation, the boiling flash is infused with steam, which
carries the oil’s vapor into the distilling head and then into the
condenser, where the oil and water co-condense. As an alternative,
steam is generated in situ in the distilling pot. By the end of the
process a mixture of water and oil will end up in the receiving flask.
The process to separate the oil from the water is difficult, we usually
use micropipettes to separate the oil as I previously stated. My
project on the other hand will be, to make a conic vassal, that will be
a substitute for the receiving flask. The vassal will have one entrance
at the bottom of the vase where the hydrolate will enter the conical
and an opening at the top with a ramp where the oil will self-extract
itself into the collection cup. The essential oil rises to the top
because it is less dense then the water plus the conical shape itself
allows for the formation of an additional separating force that helps
the rising of the oil droplets. This force is a result from the
differential between upward and downward velocities. Upward velocity
increases as the internal section of the separator turns smaller and,
on the other hand, downward velocity decreases as its diameter
increases. The conical vase will also be designed with a cylindrical
baffle on the interior to trap the incoming oil and water mixture,
which improves the separation of the oil droplets from the water.
I discovered this project by fallowing this university “Instituto
Federal de educação, ciência e tecnologia”. They did a similar project
as you can see by clicking on the link.
The whole project approximately cost me and should cost anyone who does
a similar project around $200. The majority of the materials used came
from fab lab and the distillation equipment I ordered
online.
Bill of materials:
Distillation equipment $150.23
MDF board 9mm $10
MDF board 3mm $4
ATtiny 85 $1.23
Bluetooth HC-05 $8.22 (R$32.90)
Sensor $ 6.25 (R$24.90)
ABS material $21.25 (R$85.00)
Distillation equipment:
Instead of using
the 2000 ml round bottom flask placed at the end of the distillation
equipment, I will use the essential oil extractor. I determined the
size of the conical vase by running distillation experiments with
water. The amount of liquid collected at the end of the experiment
determined the volume of the conical vase. After running the
experiment, I determined the conical vase should have a volume of
approximately 325 ml.
The Essential oil conical vase and oil collector:
I needed to change the conical vase that I made in
Computer-Aided Design week because, it was too big and I needed to add a bridge so the oil could
drain. Also I needed to add a support for the collector cup.
Below is the sketch of the new model and the diamentions:
I used
the 3D printer with ABS (Acylonitrile Butadiene Styrene) filament. It
took 18 hours to print my model.
Support table and legs:
I used plywood of 9mm for both the support table and legs and cut out the designs using the laser cutter. In
Computer-controlled cutting week
you can see more about the base and legs.
The final project by itself:
The conical vase will then be connected to the distillation equipment
by a hose that will attach at the end of the condenser and at the
entrance of the conical vase valve as you can see in the image below:
I decided to add on a system that will measure the temperature of the
oil being extracted. I chose to make a Bluetooth temperature sensor and
app to read the temperatures of the oils. The average temperature of
the essential oil was 95 F right when it was draining into the
collector.
I used the
input device combined with the
temprature sensor, which I made previously. Please take a look at those weeks to see the step by step on how I designed it.
Below are the materials I used for the Bluetooth temperature sensor:
1 x Bluetooth HC-05
1 x Power connector
1 x Audio connector (for the temperature sensor)
1 x 5V voltage regulator
2 x Capacitors
2 x 10 kΩ resistors
1 x 5 kΩ resistors
I made a box to enclose the temperature sensor board.
I designed the box using CorelDraw.
Then I cut it using the laser cutter machine using 3mm MDF, and the final result looks like this:
I put the temperature sensor inside the box and pluged in the power and temperature cables.
After I set up all the equipment and had all the materials ready, I started to grate the oranges, I used 13 oranges.
Quantity of material used:
312g orange to 1500ml water.
After I measured the weight of the 13 oranges and the water, I put both in the 2000 ml round bottom flask.
The heating mantle was switched on at an intensity 10, after 30 minutes
the mixture boiled at 192.2 F degrees and remained constant during the
process.
After boiling for 20 min, the orange peels began to rise because they
were initially below the balloon. This happens because the orange zests
density is greater than the density of the water. Distillation was
completed after 1:30 min.
After I finished extracting the essential oil I put all the oil and
water volume in a Becker to measure the oil quantity.The final volume
of oil + water was approximately 325 ml. It was observed that only 25
ml of oil was distilled, so the remaining 300 ml were of hydrolate
(water + oil mixture).
Here bellow is a picture of the full set up of the distillation equipment, the final project and the system I created.
Above is a close-up picture of the Bluetooth thermometer and app.
Initially I had used the Arduino to measure the temperature and sends
it to the bluetooth but, I had to redo the system on a board and solder
the
components of the temperature sensor
(Interface and application programming), as I described in the course of this page.
After soldering the board, I made a box to put that system inside.
In the previous photos I still had not developed the system described above.
Below are photos of the new system.
You can see the picture of the Bluetooth thermometer inside a box and the app.
At this time I didn’t use the computer because I soldered in my board a
power conector which I plugged directly into the wall outlet.
Fab license:
I chose
Fab license for my copyright.
"This work may be reproduced, modified, distributed, performed, and
displayed for any purpose, but must acknowledge "project name".
Copyright is retained and must be preserved. The work is provided as
is; no warranty is provided, and users accept all liability."
"Essential oil extractor’s a project designed By Laura Cristina
Massaglia during the Fab Academy 2017, at Fab Lab Facens, Sorocaba-SP
Brazil. It is an essential oil extractor which allows the oil to
separate by itself. This project can be modified and scaled to any size
to fulfill the needs of any project using this design and system. Since
the Essential Oil extractor is completely available on the Fab Academy
website the need for intellectual property or copyright is not at the
moment existent. Therefore, the project will be covered with a Fab Lab
license, under the name of Oil Extractor.
Here you can watch the final project video: https://youtu.be/RdERZFDrXqY
Project Files:
• Conical
• Collection cup
• Base
• Legs
• Thermometer.brd
• Thermometer.sch
• Thermometer.ino
• Bluetooth.brd
• Bluetooth.sch
• Bluetooth.ino
• App
• Link app
• Conical (Solidworks)
• Collection cup (Solidworks)
• Base (Solidworks)
• Legs (Solidworks)